HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Hydroxy-4'-nitrobiphenyl → N,N-bis-(isopropyl)-2[[4'-nitro-(1,1'-biphenyl)-4-yl]oxy]-acetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Hydroxy-4'-nitrobiphenyl | HCID 138078 | — |
| Reactant | 2-Bromo-N,N-diisopropylacetamide | HCID 10900191 | — |
| Product | N,N-bis-(isopropyl)-2[[4'-nitro-(1,1'-biphenyl)-4-yl]oxy]-acetamide | HCID 21841479 | 84.5% |
Reaction Steps
The product was prepared as in Example 2, Stage A starting with 900 mg of 4'-hydroxy-(4-nitro biphenyl) (Aldrich) and 958 mg of N,N-bis-(isopropyl)-2-bromo-acetamide (Preparation 8) to obtain 1.26 g of the expected product.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05965763 |
| Source dataset | uspto-grants-1999_10 |
| ORD ID | ord-e8bb6fd12faa4720a37a7513ab98399d |
| Source note | uspto-grants-1999_10 |