Sodium Hydroxide → HCID 21837516, compound

HRID 1739794Notes

Reaction equation

HRID 1739794 reaction equation
C[O:2][C:3]([C:5]1[C:10]2[S:11][CH2:12][CH2:13][O:14][C:9]=2[CH:8]=[CH:7][CH:6]=1)=[O:4].[OH-].[Na+]>CO>[O:14]1[C:9]2=[CH:8][CH:7]=[CH:6][C:5]([C:3]([OH:4])=[O:2])=[C:10]2[S:11][CH2:12][CH2:13]1

Participants

4

Reactant 2

HCID 14798Sodium HydroxideHCID 21837555HCID 21837555, compound

Product 1

HCID 21837516HCID 21837516, compoundYield 87.1%

Reagents, catalysts & solvents 1

HCID 887MethanolSolvent

Procedure

1.6 g of the compound obtained in Step 4 are treated for 2 hours at room temperature with 8 ml of 2N sodium hydroxide solution and 8 ml of methanol. After treatment, 1.3 g of the expected acid are isolated.

Sources & evidence

ORD record
ord-579c221219eb482aa60bfac3fe353b85
Source dataset
uspto-grants-1999_10
Patent number
US05968954

Reaction notes

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