1-Fluoro-2-nitrobenzene → HCID 21836787, compound

HRID 1740220Notes

Reaction equation

HRID 1740220 reaction equation
[CH3:1][C:2]1[CH:7]=[CH:6][C:5]([C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][C:9]=2[OH:14])=[CH:4][CH:3]=1.F[C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][C:17]=1[N+:22]([O-:24])=[O:23]>>[CH3:1][C:2]1[CH:3]=[CH:4][C:5]([C:8]2[CH:13]=[CH:12][CH:11]=[CH:10][C:9]=2[O:14][C:16]2[CH:21]=[CH:20][CH:19]=[CH:18][C:17]=2[N+:22]([O-:24])=[O:23])=[CH:6][CH:7]=1

Participants

3

Reactant 2

HCID 738951-Fluoro-2-nitrobenzeneHCID 11298348HCID 11298348, compound

Product 1

HCID 21836787HCID 21836787, compound

Procedure

Prepared from 4-methyl-2'-hydroxy-1,1'-biphenyl (Example 12, Step C) and 1-fluoro-2-nitrobenzene by the procedure described in Example 27, Step A. 1H NMR (200 MHz,CDCl3): δ 2.30 (s,3H), 6.74 (dd;2,8 Hz;1H), 6.9-7.5 (m,10H), 7.84 (dd;2,8 Hz;1H).

Sources & evidence

ORD record
ord-4aeca2ad2a134a6aa518ea53c3a075dc
Source dataset
uspto-grants-1999_10
Patent number
US05968924

Reaction notes

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