Dichloroacetic Acid → HCID 15338400, compound

HRID 1740264Notes

Reaction equation

HRID 1740264 reaction equation
Br[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][Br:14].[Cl:15][CH:16]([Cl:20])[C:17]([OH:19])=[O:18]>>[Br:14][CH2:13][CH2:12][CH2:11][CH2:10][CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2][C:16]([Cl:20])([Cl:15])[C:17]([OH:19])=[O:18]

Participants

3

Reactant 2

HCID 6597Dichloroacetic AcidHCID 187661,12-Dibromododecane

Product 1

HCID 15338400HCID 15338400, compound

Procedure

Analogously to example 1 from 50.0 g (152 mmol) 1, 12-dibromododecane and 39.3 g (305 mmol) dichloroacetic acid. Yield 11.9 g (21%), melting point 59-60° C.

Sources & evidence

ORD record
ord-aed745dfe99548d8bd365d630a2155cb
Source dataset
uspto-grants-1999_10
Patent number
US05968982

Reaction notes

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