Dichloroacetic Acid → HCID 15338402, compound

HRID 1740266Notes

Reaction equation

HRID 1740266 reaction equation
Br[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][Br:16].[Cl:17][CH:18]([Cl:22])[C:19]([OH:21])=[O:20]>>[Br:16][CH2:15][CH2:14][CH2:13][CH2:12][CH2:11][CH2:10][CH2:9][CH2:8][CH2:7][CH2:6][CH2:5][CH2:4][CH2:3][CH2:2][C:18]([Cl:22])([Cl:17])[C:19]([OH:21])=[O:20]

Participants

3

Reactant 2

HCID 6597Dichloroacetic AcidHCID 169955Tetradecane, 1,14-dibromo-

Product 1

HCID 15338402HCID 15338402, compound

Procedure

Analogously to example 1 from 2.0 g (5.6 mmol) 1,14-dibromotetradecane and 2.3 g (22.5 mmol) dichloroacetic acid. Yield 0.58 g (23%), melting point 61-63° C.

Sources & evidence

ORD record
ord-a981c5ce80be435599937c8e1161e96f
Source dataset
uspto-grants-1999_10
Patent number
US05968982

Reaction notes

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