HuagongsheHuagongshe Chemistry Print Report · For research reference only
Oxalyl chloride → HCID 17887421, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Oxalyl chloride | HCID 65578 | — |
| Reactant | HCID 10834505 | HCID 10834505 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 17887421 | HCID 17887421 | 56.8% |
Reaction Steps
1.98 g (5 mmol) 16 was stirred for 2 hours at 40° C. with 1.27 g (10 mmol) oxalyl chloride in 20 ml absolute methanol analogously to 103 (example 54). 1.1 g (57) 57 was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05968982 |
| Source dataset | uspto-grants-1999_10 |
| ORD ID | ord-016dc65062b94c04aca08541aa0b63cb |
| Source note | uspto-grants-1999_10 |