関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|
| 反応物 | 1-Bromo-3-chloropropane | HCID 8006 | — |
| 反応物 | N,N-Dimethylhexylamine | HCID 78090 | — |
| 溶媒 | Methanol | HCID 887 | — |
| 生成物 | HCID 85711135 | HCID 85711135 | — |
反応手順
A 500 mL, 3-necked, round-bottomed flask equipped with air condensers and a magnetic stirring plate was charged with N,N-dimethylhexylamine (199.46 grams, 1.54 moles), 1-bromo-3-chloropropane (243.00 grams, 1.54 moles) and 250 mL of methanol. The reaction was maintained at 65° C. for 24 hours. Solvent was removed by rotary evaporation under reduced pressure to yield a brown, viscous oil. Yield 445.8 grams (1.55 moles, 100%).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 特許番号 | US05969090 |
|---|
| 出典データセット | uspto-grants-1999_10 |
|---|
| ORD ID | ord-041ae228686d4fae866668dc87ba5254 |
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| 出典メモ | uspto-grants-1999_10 |
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