HRID1740384
反应详情
EQUATION
反应方程式
REACTANTS
反应物
PRODUCTS
生成物
AUXILIARIES
试剂、催化剂与溶剂
PROCEDURE
实验过程
A solution of 1.41 g of 1-(4-chlorophenyl)-3-(4-(2-methoxyethyl)piperazin-1-yl)methyl-2-pyrrolidinone in 10 mL of methanol was acidified by adding 4N hydrochloric acid/1,4-dioxane. The precipitated crystals were collected by filtration, washed with diethyl ether and dried in vacuo to give 1.62 g of the title compound.
WORKUP
后处理
- filtrationThe precipitated crystals were collected by filtration
- washwashed with diethyl ether
- customdried in vacuo