HRID1740384

反应详情

EQUATION

反应方程式

HRID 1740384 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A solution of 1.41 g of 1-(4-chlorophenyl)-3-(4-(2-methoxyethyl)piperazin-1-yl)methyl-2-pyrrolidinone in 10 mL of methanol was acidified by adding 4N hydrochloric acid/1,4-dioxane. The precipitated crystals were collected by filtration, washed with diethyl ether and dried in vacuo to give 1.62 g of the title compound.

WORKUP

后处理

  1. filtrationThe precipitated crystals were collected by filtration
  2. washwashed with diethyl ether
  3. customdried in vacuo