HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 10970201, compound → HCID 86754636, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 10970201 | HCID 10970201 | — |
| Reactant | 1,4-Dioxane hydrochloride | HCID 20443148 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86754636 | HCID 86754636 | — |
Reaction Steps
A solution of 1.0 g of (S)-1-(4-chlorophenyl)-3-(4-(2-methoxyethyl)piperazin-1-yl)methyl-2-pyrrolidinone in 50 mL of ethanol was acidified with 4N hydrochloric acid/1,4-dioxane. The precipitated crystals were filtered, washed with diethyl ether and dried in vacuo to give 1.18 g of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05969138 |
| Source dataset | uspto-grants-1999_10 |
| ORD ID | ord-9da670f67b50472a9d26842652c0a885 |
| Source note | uspto-grants-1999_10 |