HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Amino-5,5-dimethyl-2-cyclohexen-1-one → HCID 22117811, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Amino-5,5-dimethyl-2-cyclohexen-1-one | HCID 136680 | — |
| Reactant | 4-Chloro-3-Fluorobenzaldehyde | HCID 2724985 | — |
| Product | HCID 22117811 | HCID 22117811 | — |
Reaction Steps
Reaction of 3-amino-5,5-dimethyl-2-cyclohexen-1-one with 4-chloro-3-fluorobenzaldehyde in an analogous manner to that described in Example 1 gave 9-(4-chloro-3-fluorophenyl)-3,4,6,7,9,10-hexahydro-3,3,6,6-tetramethyl-1,8(2H,5H)-acridinedione. Crystallization from absolute ethanol gave a yellow crystalline solid of melting point >300° C. (decomposition).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05969139 |
| Source dataset | uspto-grants-1999_10 |
| ORD ID | ord-d1e476b7009045518c8187bc95af4334 |
| Source note | uspto-grants-1999_10 |