HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Amino-5,5-dimethyl-2-cyclohexen-1-one → HCID 9804996, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Amino-5,5-dimethyl-2-cyclohexen-1-one | HCID 136680 | — |
| Reactant | HCID 15300641 | HCID 15300641 | — |
| Product | HCID 9804996 | HCID 9804996 | — |
Reaction Steps
Reaction of 3-amino-5,5-dimethyl-2-cyclohexen-1-one with 4-chloro-3-phenoxybenzaldehyde in an analogous manner to that described in Example 1 gave 9-(4-chloro-3-phenoxyphenyl)-3,4,6,7,9,10-hexahydro-3,3,6,6-tetramethyl-1,8(2H,5H)-acridinedione. Crystallization from dimethylformamide/water gave a yellow crystalline solid of melting point 246-248° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05969139 |
| Source dataset | uspto-grants-1999_10 |
| ORD ID | ord-0214b1c9403146eeab972e6bfcc63d4f |
| Source note | uspto-grants-1999_10 |