3-(4-Methoxyphenoxy)benzaldehyde → HCID 22117853, compound

HRID 1740452Notes

Reaction equation

HRID 1740452 reaction equation
[NH2:1][C:2]1[CH2:7][C:6]([CH3:9])([CH3:8])[CH2:5][C:4](=[O:10])[CH:3]=1.[CH3:11][O:12][C:13]1[CH:27]=[CH:26][C:16]([O:17][C:18]2[CH:19]=[C:20]([CH:23]=[CH:24][CH:25]=2)[CH:21]=O)=[CH:15][CH:14]=1>>[CH3:8][C:6]1([CH3:9])[CH2:7][C:2]2[NH:1][C:2]3[CH2:7][C:6]([CH3:9])([CH3:8])[CH2:5][C:4](=[O:10])[C:3]=3[CH:21]([C:20]3[CH:23]=[CH:24][CH:25]=[C:18]([O:17][C:16]4[CH:26]=[CH:27][C:13]([O:12][CH3:11])=[CH:14][CH:15]=4)[CH:19]=3)[C:3]=2[C:4](=[O:10])[CH2:5]1

Participants

3

Reactant 2

HCID 1235533-(4-Methoxyphenoxy)benzaldehydeHCID 1366803-Amino-5,5-dimethyl-2-cyclohexen-1-one

Product 1

HCID 22117853HCID 22117853, compound

Procedure

3-Amino-5,5-dimethyl-2-cyclohexen-1-one was reacted with 3-(4-methoxyphenoxy)-benzaldehyde in an analogous manner to that described in Example 1 to give 3,4,6,7,9,10-hexahydro-3,3,6,6-tetramethyl-9- [3-(4-methoxyphenoxy)-phenyl]-1,8(2H,5H)-acridinedione. Crystallization from ethanol/water gave a pale yellow crystalline solid of melting point 210-212° C.

Sources & evidence

ORD record
ord-aa54252a0979460786bcb05cd57faba5
Source dataset
uspto-grants-1999_10
Patent number
US05969139

Reaction notes

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