3-Amino-5,5-dimethyl-2-cyclohexen-1-one → HCID 22117862, compound

Participants

Reaction Steps

3-Amino-5,5-dimethyl-2-cyclohexen-1-one was reacted with 3-(4-chlorophenoxy)benzaldehyde in an analogous manner to that described in Example 1 to give 9-[3-(4-chlorophenoxy)-phenyl]-3,4,6,7,9,10-hexahydro-3,3,6,6-tetramethyl-1,8(2H,5H)-acridinedione. Crystallization from dimethylformamide/water gave a beige crystalline solid of melting point 238-239° C.

Provenance & Evidence