3-Amino-5,5-dimethyl-2-cyclohexen-1-one → HCID 22117850, compound

HRID 1740456Notes

Reaction equation

HRID 1740456 reaction equation
[NH2:1][C:2]1[CH2:7][C:6]([CH3:9])([CH3:8])[CH2:5][C:4](=[O:10])[CH:3]=1.[C:11]([O:19][C:20]1[CH:21]=[C:22]([CH:25]=[CH:26][CH:27]=1)[CH:23]=O)(=[O:18])[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1>>[C:11]([O:19][C:20]1[CH:21]=[C:22]([CH:23]2[C:3]3[C:4](=[O:10])[CH2:5][C:6]([CH3:9])([CH3:8])[CH2:7][C:2]=3[NH:1][C:2]3[CH2:7][C:6]([CH3:9])([CH3:8])[CH2:5][C:4](=[O:10])[C:3]2=3)[CH:25]=[CH:26][CH:27]=1)(=[O:18])[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1

Participants

3

Reactant 2

HCID 1366803-Amino-5,5-dimethyl-2-cyclohexen-1-oneHCID 569516HCID 569516, compound

Product 1

HCID 22117850HCID 22117850, compound

Procedure

3-Amino-5,5-dimethyl-2-cyclohexen-1-one was reacted with 3-benzoyloxybenzaldehyde in an analogous manner to that described in Example 1 to give 9-(3-benzoyloxyphenyl)-3,4,6,7,9,10-hexahydro-3,3,6,6-tetramethyl-1,8(2H,5H)-acridinedione. Crystallization from ethanol gave a pale yellow crystalline solid of melting point 274-275° C. (decomposition).

Sources & evidence

ORD record
ord-2c4a7c6f00a94288927004fae9433f26
Source dataset
uspto-grants-1999_10
Patent number
US05969139

Reaction notes

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