Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ethylene Glycol | HCID 174 | — |
| Reactant | Dichloromethane | HCID 6344 | — |
| Reactant | Phthalic Anhydride | HCID 6811 | — |
| Reactant | HCID 22007376 | HCID 22007376 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 178486627 | HCID 178486627 | 61.5% |
Reaction Steps
A mixture of 1-(2-hydrazino-4-pyridyl)-2,3-bis(hydroxymethyl)-6,7-dimethoxynaphthalene (2.0 g), phthalic anhydride (0.92 g) and ethylene glycol (10 ml) is heated with stirring at 130° C. for two hours. The mixture is cooled to room temperature, and thereto are added methylene chloride and water. The methylene chloride layer is separated, washed, dried, concentrated under reduced pressure to remove the solvent, and the residue is crystallized from ethanol to give 1-[2-{4-(hydroxy)-1(2H)-phthalazinon-2-yl}-4-pyridyl]-2,3-bis(hydroxymethyl)-6,7-dimethoxynaphthalene (1.68 g, yield; 61%), which is listed in Table 10.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US05969140 |
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| Source dataset | uspto-grants-1999_10 |
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| ORD ID | ord-1d7f45e66da340bd8306c0f7b15b7e2e |
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| Source note | uspto-grants-1999_10 |
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