HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,4-Oxazolidinedione → HCID 57269904, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,4-Oxazolidinedione | HCID 97389 | — |
| Reactant | HCID 10497550 | HCID 10497550 | — |
| Product | HCID 57269904 | HCID 57269904 | 44% |
Reaction Steps
In substantially the same manner as in Example 1, (E)-3-[2-(5-methyl-2-phenyl-4-oxazolylmethyl)benzofuran-5-yl]acrolein was allowed to react with 2,4-oxazolidinedione to give 5-[3-[2-(5-methyl-2-phenyl-4-oxazolylmethyl)benzofuran-5-yl]-2-propenylidene]-2,4-oxazolidinedione. The yield was 44%. Recrystallization from dichloromethane-methanol gave pale yellow needles, m.p.237-239° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05972970 |
| Source dataset | uspto-grants-1999_10 |
| ORD ID | ord-07b650a1a851406bb0455c1651320f4a |
| Source note | uspto-grants-1999_10 |