HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → Phenyl-3-chlorobenzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Phenol | HCID 996 | — |
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | Benzoyl chloride, 3-chloro- | HCID 69252 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | Phenyl-3-chlorobenzoate | HCID 11984386 | — |
Reaction Steps
Phenyl-3-chlorobenzoate is prepared by reacting 3-chlorobenzoyl chloride with phenol in toluene with some pyridine (1 mol equivalent per acid chloride) to trap the HCl that evolves. After aqueous extraction of the pyridinium salt and any excess starting materials, the product is crystallized from the toluene solution.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05973075 |
| Source dataset | uspto-grants-1999_10 |
| ORD ID | ord-915fb2ca6d894b23bc39ae7dc428a140 |
| Source note | uspto-grants-1999_10 |