Pyridine → HCID 23303938, compound

Participants

Reaction Steps

A solution of 3.0 g (24 mmol) of methyl phenyl sulfide in 30 mL of dichloromethane was cooled to -10° C. and 1.7 g (24 mmol) of chlorine was sparged in with cooling and stirring. To this was added with cooling and stirring 4.5 g (24 mmol) of solid methyl 6-chloroanthranilate and then 3.8 g (48 mmol) of pyridine. The product mixture contained the title compound and methyl 6-chloroanthranilate in a 60:40 ratio as determined by HPLC.

Provenance & Evidence