HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triphenylphosphine → HCID 86751799, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triphenylphosphine | HCID 11776 | — |
| Reactant | ethyl N-ethoxycarbonyliminocarbamate | HCID 220568 | — |
| Reactant | 5-(4-Hydroxybenzyl)-3-triphenylmethylthiazolidine-2,4-dione | HCID 2818126 | — |
| Reactant | HCID 53783169 | HCID 53783169 | — |
| Product | HCID 86751799 | HCID 86751799 | 76.2% |
Reaction Steps
Following a procedure similar to that described in Example 1(a), but using 483 mg of 2-(3-phenylbenzylideneaminooxy)ethanol (prepared as described in Preparation 8), 716 mg of 5-(4-hydroxybenzyl)-3-tritylthiazolidine-2,4-dione, 525 mg of triphenylphosphine and 348 mg of diethyl azodicarboxylate, 807 mg of the title compound were obtained as a foam-like solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05972959 |
| Source dataset | uspto-grants-1999_10 |
| ORD ID | ord-fd214da89a784dc78a9c3a81ab025869 |
| Source note | uspto-grants-1999_10 |