HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → Methyl 3-[2-[2-(4-fluorophenyl)ethoxy]ethylaminosulphonyl]propanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | Methyl 3-(chlorosulfonyl)propanoate | HCID 4962888 | — |
| Reactant | 2-[(4-Fluorophenethyl)oxy]ethylamine | HCID 18779064 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | Methyl 3-[2-[2-(4-fluorophenyl)ethoxy]ethylaminosulphonyl]propanoate | HCID 18779017 | 85.3% |
Reaction Steps
The subtitle compound (8.32 g) was prepared according to the method of Example 3d) using 2-[2-(4-fluorophenyl)ethoxy]ethanamine (5.36 g), triethylamine (4.6 ml) and methyl 3-(chlorosulphonyl)propanoate (5.6 g) in diethyl ether (150 ml).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05973167 |
| Source dataset | uspto-grants-1999_10 |
| ORD ID | ord-69253e3181a24c7197fc997cedde9ca0 |
| Source note | uspto-grants-1999_10 |