HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisobutylaluminum hydride → 3-(2-Pyridyl)-2-propen-1-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisobutylaluminum hydride | HCID 14487 | — |
| Reactant | HCID 5371891 | HCID 5371891 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 3-(2-Pyridyl)-2-propen-1-ol | HCID 13864855 | — |
Reaction Steps
As in Example 3, Step 2, but using a 1.5M solution of DIBAL in toluene, the ester from Step 1 of the present example was converted to the title compound. The alcohol was chromatographed on silica using EtOAc/toluene (9:1) as eluent.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05334597 |
| Source dataset | uspto-grants-1994_08 |
| ORD ID | ord-8c2846b9ad0c48d890b85d4f80be9722 |
| Source note | uspto-grants-1994_08 |