Sodium Hydroxide → HCID 19010498, compound

Participants

Reaction Steps

A 5N sodium hydroxide solution (0.1 mL) was added to a stirred mixture of the product of Step A (22 mg, 0.0410 mmol) in methanol (1mL). A few drops of methylene chloride were added to allow stirring then the mixture was stirred at room temperature for 2.5 h. The solvent was removed in vacuo then 5% citric acid solution added. The precipitate was filtered off, washed with water and dried in vacuo to give the titled carboxylic acid (18 mg).

Provenance & Evidence