HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → 2-Chloro-4-ethoxy-6-methoxy-1,3,5-triazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | 2,4-Dichloro-6-methoxy-3,5-triazine | HCID 19267 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | 2-Chloro-4-ethoxy-6-methoxy-1,3,5-triazine | HCID 19010699 | — |
Reaction Steps
The 2,4-dichloro-6-methoxy-s-triazine obtained as described in Example A-3 is suspended in acetone, 46 parts of ethanol and 90 parts of sodium bicarbonate are slowly added, and the reaction is carried out at a temperature of between 40° and 50° C. for about one hour. The mixture is then evaporated to give the compound 2-chloro-4-methoxy-6-ethoxy-s-triazine as a powder which contains electrolyte salts and serves as the monochloro-triazine starting compound in the synthesis of dyestuffs according to the invention.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05334709 |
| Source dataset | uspto-grants-1994_08 |
| ORD ID | ord-b0d7ee1ce1fc467d81f5052c2ee11577 |
| Source note | uspto-grants-1994_08 |