HuagongsheHuagongshe Chemistry Print Report · For research reference only
ethyl (4E)-5-(2-pyridyl)-4-pentenoate → Ethyl 5-(pyridin-2-yl)pentanoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | ethyl (4E)-5-(2-pyridyl)-4-pentenoate | HCID 11217977 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | Ethyl 5-(pyridin-2-yl)pentanoate | HCID 11241218 | 99% |
Reaction Steps
To a solution of ethyl (4E)-5-(2-pyridyl)-4-pentenoate (1.84 g) in ethanol (15 ml) was added 10% palladium on carbon (145 mg), and the mixture was stirred for 3 hours under an atmosphere of hydrogen (4 atm), and then filtered through a celite pad. Removal of the solvent in vacuo gave ethyl 5-(2-pyridyl)pentanoate (1.84 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05334716 |
| Source dataset | uspto-grants-1994_08 |
| ORD ID | ord-311dbe55b5d645dd9b512fd76a1be2f3 |
| Source note | uspto-grants-1994_08 |