Cyclopentadecanone → N-Cyclopentadecyl-N-(3-pyridylmethyl)amine

HRID 1741934Notes

Reaction equation

[NH2:1][CH2:2][C:3]1[CH:4]=[N:5][CH:6]=[CH:7][CH:8]=1.[C:9]1(=O)[CH2:23][CH2:22][CH2:21][CH2:20][CH2:19][CH2:18][CH2:17][CH2:16][CH2:15][CH2:14][CH2:13][CH2:12][CH2:11][CH2:10]1>>[CH:9]1([NH:1][CH2:2][C:3]2[CH:4]=[N:5][CH:6]=[CH:7][CH:8]=2)[CH2:23][CH2:22][CH2:21][CH2:20][CH2:19][CH2:18][CH2:17][CH2:16][CH2:15][CH2:14][CH2:13][CH2:12][CH2:11][CH2:10]1

Participants

Reactant 2

HCID 10409Cyclopentadecanone

HCID 310183-Pyridinemethanamine

Product 1

HCID 14800148N-Cyclopentadecyl-N-(3-pyridylmethyl)amine

Procedure

Following the general procedure of Example 33, but starting with 3-aminomethylpyridine and cyclopentadecanone, the rifle compound is produced, NMR (CDCl3, TMS) δ8.58, 7.72, 7.25, 3.76, 2.56, 1.32.

Workup

customthe rifle compound is produced

Sources & evidence

ORD record: ord-bdb2fac494ec46479e7434a3994789b2
Source dataset: uspto-grants-1994_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05334712

Reaction notes

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