HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(2-{[(Tert-butoxy)carbonyl]amino}acetamido)acetic acid → Boc-Gly-Gly-Val-Pro-OH
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(2-{[(Tert-butoxy)carbonyl]amino}acetamido)acetic acid | HCID 333466 | — |
| Reactant | Boc-Gly-Gly-Val-Pro-OBzl | HCID 14306249 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | Boc-Gly-Gly-Val-Pro-OH | HCID 14306251 | — |
Reaction Steps
IV (6.2 g, 0.012 mole) in acetic acid was hydrogenated and worked up as for II to obtain V quantitatively, no sharp m.p. 74°-83° C. Rf3, 0.25; Rf4, 0.15. Anal. Calcd. for C19H32N4O7 : C, 51.10; H, 7.67; N, 12.54%. Found: C, 51.28: H, 7.50 N, 12.38%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05336256 |
| Source dataset | uspto-grants-1994_08 |
| ORD ID | ord-cf8016fb33014f40a3f567f1104ecd56 |
| Source note | uspto-grants-1994_08 |