Phenanthridine → HCID 178479920, compound

HRID 1742003Notes

Reaction equation

HRID 1742003 reaction equation
[OH:1][CH2:2][SnH2:3][C:4]1[C:17]2[C:8](=[N:9][CH:10]=[C:11]3[C:16]=2[CH:15]=[CH:14][CH:13]=[CH:12]3)[CH:7]=[CH:6][CH:5]=1.[CH:18]1C2C(=NC=C3C=2C=CC=C3)C=CC=1>>[CH3:18][N:9]1[CH2:10][C:11]2[C:16](=[CH:15][CH:14]=[CH:13][CH:12]=2)[C:17]2[C:4]([SnH2:3][CH2:2][OH:1])=[CH:5][CH:6]=[CH:7][C:8]1=2

Participants

3

Reactant 2

HCID 9189PhenanthridineHCID 131718636HCID 131718636, compound

Product 1

HCID 178479920HCID 178479920, compound

Procedure

Employing the procedure described in Example 2, but substituting the hydroxymethylphenanthridinyl stannane 35 prepared as described in Example 30 for the stannane 2, provides the N-methyl hydroxymethylphenanthridinyl stannane 36.

Workup

  1. customprepared

Sources & evidence

ORD record
ord-5483d63f4eb04510a9ce65010ac77112
Source dataset
uspto-grants-1994_08
Patent number
US05336674

Reaction notes

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