HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Di-tert-butyl-4-methylphenol → HCID 10713635, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Di-tert-butyl-4-methylphenol | HCID 31404 | — |
| Reactant | Chlorosulfonyl isocyanate | HCID 70918 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 10713635 | HCID 10713635 | 74.1% |
Reaction Steps
A solution of 2,6-di-t-butyl-4-methylphenol (22.04 g, 0.1 moles) in 100 mL Et2O was added dropwise to a solution of chlorosulfonyl isocyanate (8.7 mL, 0.1 moles) in 100 mL Et2O at -15° C. under an atmosphere of N2. This was stirred for 2 hours, concentrated and trituration of the resulting gel with hexanes gave 26.82 g (74%) of the title compound as a white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05336690 |
| Source dataset | uspto-grants-1994_08 |
| ORD ID | ord-c9cb3a325293470687abc0707a6254d0 |
| Source note | uspto-grants-1994_08 |