Sodium borohydride → HCID 19009255, compound

HRID 1742502Notes

Reaction equation

HRID 1742502 reaction equation
[CH3:1][O:2][C:3]1[C:12]2[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=2)[C:6]([O:13][CH3:14])=[CH:5][C:4]=1[CH2:15][CH2:16][CH2:17][CH:18]=[O:19].[BH4-].[Na+]>C(O)C>[CH3:1][O:2][C:3]1[C:12]2[C:7](=[CH:8][CH:9]=[CH:10][CH:11]=2)[C:6]([O:13][CH3:14])=[CH:5][C:4]=1[CH2:15][CH2:16][CH2:17][CH2:18][OH:19]

Participants

4

Reactant 2

HCID 4311764Sodium borohydrideHCID 19009260HCID 19009260, compound

Product 1

HCID 19009255HCID 19009255, compoundYield 95.2%

Reagents, catalysts & solvents 1

HCID 702EthanolSolvent

Procedure

Following a procedure similar to that described in Preparation 1(c), but using 2.96 g of 4-(1,4-dimethoxy-2-naphthyl)butyraldehyde [prepared as described in step (b) above], 0.87 g of sodium borohydride and 80 ml of ethanol, 2.84 g of the title compound were obtained as a colorless oil.

Sources & evidence

ORD record
ord-ddf14f110304459d9f2aada95c9f7d68
Source dataset
uspto-grants-1994_08
Patent number
US05338855

Reaction notes

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