Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2,4,6-Trimethylaniline → 2-Methyl-6,11-dihydro-dibenzo[b,e]oxepine-11-carboxylic acid (2,4,6-trimethyl-phenyl)-amide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2,4,6-Trimethylaniline | HCID 6913 | — |
| 반응물 | 6,11-Dihydro-2-methyldibenz[b,e]-oxepin-11-carboxylic acid | HCID 10106342 | — |
| 생성물 | 2-Methyl-6,11-dihydro-dibenzo[b,e]oxepine-11-carboxylic acid (2,4,6-trimethyl-phenyl)-amide | HCID 10429309 | 61.5% |
반응 단계
The similar procedures as in Example 1 were repeated except using 1.47 g of Compound A and 0.71 g of 2,4,6-trimethylaniline in place of aniline to obtain 1.20 g of Compound 9.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05340807 |
| 출처 데이터셋 | uspto-grants-1994_08 |
| ORD ID | ord-4a25c35db4f3427c8d7e30e5ecad137c |
| 출처 메모 | uspto-grants-1994_08 |