2,6-Diethylaniline → HCID 10024754, compound

HRID 1742644Notes

Reaction equation

HRID 1742644 reaction equation
[CH:1]([C:4]1[CH:21]=[CH:20][C:7]2[O:8][CH2:9][C:10]3[CH:19]=[CH:18][CH:17]=[CH:16][C:11]=3[CH:12]([C:13](O)=[O:14])[C:6]=2[CH:5]=1)([CH3:3])[CH3:2].[CH2:22]([C:24]1[CH:30]=[CH:29][CH:28]=[C:27]([CH2:31][CH3:32])[C:25]=1[NH2:26])[CH3:23]>>[CH2:22]([C:24]1[CH:30]=[CH:29][CH:28]=[C:27]([CH2:31][CH3:32])[C:25]=1[NH:26][C:13]([CH:12]1[C:11]2[CH:16]=[CH:17][CH:18]=[CH:19][C:10]=2[CH2:9][O:8][C:7]2[CH:20]=[CH:21][C:4]([CH:1]([CH3:3])[CH3:2])=[CH:5][C:6]1=2)=[O:14])[CH3:23]

Participants

3

Reactant 2

HCID 113692,6-DiethylanilineHCID 9993912HCID 9993912, compound

Product 1

HCID 10024754HCID 10024754, compoundYield 50.5%

Procedure

The similar procedures as in Example 1 were repeated except using 2.34 g of Compound C in place of Compound A and 0.90 g of 2,6-diethylaniline in place of aniline to obtain 1.26 g of Compound 13.

Sources & evidence

ORD record
ord-dd895b2e7a8c482d90eb71518e9d6783
Source dataset
uspto-grants-1994_08
Patent number
US05340807

Reaction notes

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