HuagongsheHuagongshe Chemistry Print Report · For research reference only
6,11-Dihydro-2-methyldibenz[b,e]-oxepin-11-carboxylic acid → 6,11-Dihydro-N-(2,6-diisopropyl-4-thiocyanatophenyl)-2-methyldibenz[b,e]oxepin-11-carboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6,11-Dihydro-2-methyldibenz[b,e]-oxepin-11-carboxylic acid | HCID 10106342 | — |
| Reactant | 4-Amino-3,5-di(propan-2-yl)phenyl thiocyanate | HCID 18998488 | — |
| Product | 6,11-Dihydro-N-(2,6-diisopropyl-4-thiocyanatophenyl)-2-methyldibenz[b,e]oxepin-11-carboxamide | HCID 18998484 | 78.6% |
Reaction Steps
The similar procedures as in Example 1 were repeated except using 1.12 g of Compound A and 1.24 g of 2,6-diisopropyl-4-thiocyanatoaniline in place of aniline to obtain 1.63 g of Compound 31.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05340807 |
| Source dataset | uspto-grants-1994_08 |
| ORD ID | ord-2bcc9b1db15a40daa15556a1a3c05b65 |
| Source note | uspto-grants-1994_08 |