HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromo-6,11-dihydrodibenz[b,e]oxepin-11-carboxylic acid → 2-Bromo-6,11-dihydro-N-(2,6-diisopropyl-4-methylthiophenyl)dibenz[b,e]oxepin-11-carboxamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromo-6,11-dihydrodibenz[b,e]oxepin-11-carboxylic acid | HCID 10403641 | — |
| Reactant | 2,6-Diisopropyl-4-methylthioaniline | HCID 18998505 | — |
| Product | 2-Bromo-6,11-dihydro-N-(2,6-diisopropyl-4-methylthiophenyl)dibenz[b,e]oxepin-11-carboxamide | HCID 18998509 | 76.1% |
Reaction Steps
The similar procedures as in Example 1 were repeated except using 1.0 g of 2-bromo-6,11-dihydrodibenz[b,e]oxepin-11-carboxylic acid obtained in Example 46 (Compound H) in place of Compound A and 0.84 g of 2,6-diisopropyl-4-methylthioaniline in place of aniline to obtain 1.25 g of Compound 44.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05340807 |
| Source dataset | uspto-grants-1994_08 |
| ORD ID | ord-93fb24f133d74cd2aded814a71bc6750 |
| Source note | uspto-grants-1994_08 |