2,6-Diethylaniline → HCID 18998489, compound

HRID 1742662Notes

Reaction equation

HRID 1742662 reaction equation
[CH3:1][C:2]1[C:12]2[CH:11]([C:13](O)=[O:14])[C:10]3[CH:16]=[CH:17][CH:18]=[CH:19][C:9]=3[CH2:8][O:7][C:6]=2[C:5]([CH3:20])=[CH:4][CH:3]=1.[CH2:21]([C:23]1[CH:29]=[CH:28][CH:27]=[C:26]([CH2:30][CH3:31])[C:24]=1[NH2:25])[CH3:22]>>[CH2:21]([C:23]1[CH:29]=[CH:28][CH:27]=[C:26]([CH2:30][CH3:31])[C:24]=1[NH:25][C:13]([CH:11]1[C:10]2[CH:16]=[CH:17][CH:18]=[CH:19][C:9]=2[CH2:8][O:7][C:6]2[C:5]([CH3:20])=[CH:4][CH:3]=[C:2]([CH3:1])[C:12]1=2)=[O:14])[CH3:22]

Participants

3

Reactant 2

HCID 113692,6-DiethylanilineHCID 18998494HCID 18998494, compound

Product 1

HCID 18998489HCID 18998489, compoundYield 41%

Procedure

The similar procedures as in Example 1 were repeated except using 1.0 g of 6, 11-dihydro-1,4-dimethyldibenz[b,e]oxepin-11-carboxylic acid obtained in Example 64 (Compound AC) in place of Compound A and 0.62 g of 2,6-diethylaniline in place of aniline to obtain 0.61 g of Compound 50.

Sources & evidence

ORD record
ord-2516dde9181e4c24a7d2833b0227864e
Source dataset
uspto-grants-1994_08
Patent number
US05340807

Reaction notes

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