Tetrahydrofuran → HCID 86748088, compound

Participants

Reaction Steps

Into a similar reaction vessel, as used in the abovementioned reaction, were placed 1.342 parts of t-BuOK and 7.607 parts of THF and to this, a mixture of 10.000 parts of 1propargyloxybiphenyl and 23.333 parts of THF was added dropwise. The content was reacted at 50° C. for 60 minutes and then a deionized water was added to stop the reaction. THF layer and water layer were removed by using an evaporator, and the residue was subjected to a column chromatography (silica gel 200 mesh) to obtain a purified 1-allenyloxy biphenyl as colorless oily product. This compound was identified by FT-NMR(H) and IR spectrum. The reaction yield was 63.2%.

Provenance & Evidence