Tetrahydrofuran → HCID 14597333, compound

Participants

Reaction Steps

Into a similar reaction vessel, as used in the abovementioned reaction, were placed 2.316 parts of t-BuOK and 13.108 parts of THF and to this, a mixture of 10,000 parts of 2,7-dipropargyloxynaphthalene and 23.333 parts of THF was added dropwise. The content was reacted at 50° C. for 60 minutes and then a deionized water was added to stop the reaction. THF layer and water layer were removed off by using an evaporator, and the residue was subjected to a column chromatography (silica gel 200 mesh) to obtain a purified 2,7-diallenyloxy naphthalene as white rystals (M.P. 80.5°-83.5° C.)

Provenance & Evidence