Tetrahydrofuran → HCID 14597330, compound

Participants

Reaction Steps

Into a similar reaction vessel, as used in the abovementioned reaction, were placed 2.124 parts of t-BuOK and 12.036 parts of THF and to this, a mixture of 10.000 parts of 4,4'-dipropargyloxybiphenyl and 23.333 parts of THF was added dropwise. The content was reacted at 50° C. for 60 minutes and then a deionized water was added to stop the reaction. THF layer and water layer were removed by using an evaporator, and the residue was subjected to a column chromatography (silica gel 200 mesh) to obtain a purified 4,4'-diallenyloxy biphenyl as pale yellow crystals (M.P.135.2°-138.5° C.)

Provenance & Evidence