2-Ethylhexanol → HCID 19006784, compound

HRID 1742768Notes

Reaction equation

HRID 1742768 reaction equation
ClC1C=C(Cl)N=C(C2C=CC=CC=2)N=1.Cl[C:16]1[CH:21]=[C:20]([Cl:22])[N:19]=[C:18]([S:23][C:24]2[CH:29]=[CH:28][C:27]([CH3:30])=[CH:26][CH:25]=2)[N:17]=1.[CH2:31]([CH:33]([CH2:36][CH2:37][CH2:38][CH3:39])[CH2:34][OH:35])[CH3:32]>CC(C)CCO>[Cl:22][C:20]1[CH:21]=[C:16]([O:35][CH2:34][CH:33]([CH2:31][CH3:32])[CH2:36][CH2:37][CH2:38][CH3:39])[N:17]=[C:18]([S:23][C:24]2[CH:29]=[CH:28][C:27]([CH3:30])=[CH:26][CH:25]=2)[N:19]=1

Participants

5

Reactant 3

HCID 77202-EthylhexanolHCID 77338FenclorimHCID 19006778HCID 19006778, compound

Product 1

HCID 19006784HCID 19006784, compoundYield 85%

Reagents, catalysts & solvents 1

HCID 31260Isoamyl AlcoholSolvent

Procedure

The preparation is carried out analogously to the method described in Example 3, with 4,6-dichloro-2-phenylpyrimidine being replaced by 4,6-dichloro-2-(p-methylphenylthio)pyrimidine and 3-methylbutanol by 2-ethylhexanol. The title compound is obtained as a resin in a yield of 85% of theory.

Sources & evidence

ORD record
ord-6d3b3df2e8a44f8aa36aff2be50b81b5
Source dataset
uspto-grants-1994_08
Patent number
US05340701

Reaction notes

Loading…