HRID1743

反应详情

EQUATION

反应方程式

HRID 1743 的结构方程式

PROCEDURE

实验过程

10 g (60 mmol) of 5-hydroxy-2-nitrobenzyl alcohol were reacted with 7.0 ml (70 mmol) of isopropyl iodide analogously to Example 4a); after purification over silica gel with n-heptane/ethyl acetate (3:2), 10.3 g of oily crude product.

WORKUP

后处理

  1. customafter purification over silica gel with n-heptane/ethyl acetate (3:2), 10.3 g of oily crude product