Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-(2-Hydroxy-1-decyloxy)nitrobenzene → 4-(2-Hydroxy-1-decyloxy)aniline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-(2-Hydroxy-1-decyloxy)nitrobenzene | HCID 22237769 | — |
| 반응물 | HCID 178418361 | HCID 178418361 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 용매 | Ethyl Acetate | HCID 8857 | — |
| 생성물 | 4-(2-Hydroxy-1-decyloxy)aniline | HCID 22237771 | — |
반응 단계
4-(2-hydroxy-1-decyloxy)nitrobenzene (20 g, 0.68 mol) was dissolved in ethyl acetate (200 mL) and 10% palladium on carbon (2.5 g) was added to a Parr pressure bottle. The contents were then hydrogenated at 50 psi until hydrogen uptake ceased. The catalyst was removed by suction filtration through a pad of Celite. Removal of solvent afforded 4-(2-hydroxy-1-decyloxy)aniline in quantitative yield (18.0 g, 0.68 mol, 100% yield) as a tan solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07008759B2 |
| 출처 데이터셋 | uspto-grants-2006_03 |
| ORD ID | ord-67e43c96b08d480a98f74350ff1c82b4 |
| 출처 메모 | uspto-grants-2006_03 |