2-Butanamine, 1-methoxy- → HCID 10018721, compound

HRID 1743299Notes

Reaction equation

HRID 1743299 reaction equation
[CH2:1]([O:3][C:4]([C:6]1[CH:7]=[N:8][C:9]2[C:14]([C:15]=1Cl)=[CH:13][CH:12]=[CH:11][C:10]=2[N+:17]([O-])=O)=[O:5])[CH3:2].[CH3:20][O:21][CH2:22][CH:23]([NH2:26])[CH2:24][CH3:25]>>[CH2:1]([O:3][C:4]([C:6]1[CH:7]=[N:8][C:9]2[C:14]([C:15]=1[NH:26][CH:23]([CH2:22][O:21][CH3:20])[CH2:24][CH3:25])=[CH:13][CH:12]=[CH:11][C:10]=2[NH2:17])=[O:5])[CH3:2]

Participants

3

Reactant 2

HCID 938372-Butanamine, 1-methoxy-HCID 11196760Ethyl 4-chloro-8-nitroquinoline-3-carboxylate

Product 1

HCID 10018721HCID 10018721, compoundYield 80%

Procedure

The compound prepared in Example 3 was reacted with 1-methoxy-2-aminobutane according to the method as described in Example 4 and the obtained compound was treated as described in Example 14 to prepare the title compound (yield 80%).

Workup

  1. additionthe obtained compound was treated

Sources & evidence

ORD record
ord-f9e8147c576d46bca8011188fee01547
Source dataset
uspto-grants-2006_03
Patent number
US07009053B2

Reaction notes

Loading…