3-Phenylpropylamine → HCID 10247242, compound

HRID 1743312Notes

Reaction equation

HRID 1743312 reaction equation
[CH2:1]([O:3][C:4]([C:6]1[CH:7]=[N:8][C:9]2[C:14]([C:15]=1Cl)=[CH:13][CH:12]=[CH:11][C:10]=2[N+:17]([O-])=O)=[O:5])[CH3:2].[C:20]1([CH2:26][CH2:27][CH2:28][NH2:29])[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1>>[CH2:1]([O:3][C:4]([C:6]1[CH:7]=[N:8][C:9]2[C:14]([C:15]=1[NH:29][CH2:28][CH2:27][CH2:26][C:20]1[CH:25]=[CH:24][CH:23]=[CH:22][CH:21]=1)=[CH:13][CH:12]=[CH:11][C:10]=2[NH2:17])=[O:5])[CH3:2]

Participants

3

Reactant 2

HCID 162593-PhenylpropylamineHCID 11196760Ethyl 4-chloro-8-nitroquinoline-3-carboxylate

Product 1

HCID 10247242HCID 10247242, compoundYield 88%

Procedure

The compound prepared in Example 3 was reacted with 3-phenyl-propylamine according to the method as described in Example 4 and the obtained compound was treated as described in Example 14 to prepare the title compound (yield 88%).

Workup

  1. additionthe obtained compound was treated

Sources & evidence

ORD record
ord-ec247a162991420c9426eafd4cd427fb
Source dataset
uspto-grants-2006_03
Patent number
US07009053B2

Reaction notes

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