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2-((4-Chlorophenyl)methyl)propanedinitrile → 2-(4-Chlorobenzyl)-2-(3,3,4,4,4-pentafluorobutyl)malononitrile
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | 2-((4-Chlorophenyl)methyl)propanedinitrile | HCID 18082 | — |
| 反応物 | Sodium hydride | HCID 24758 | — |
| 反応物 | 1,1,1,2,2-Pentafluoro-4-iodobutane | HCID 110092 | — |
| 溶媒 | Dimethylformamide | HCID 6228 | — |
| 生成物 | 2-(4-Chlorobenzyl)-2-(3,3,4,4,4-pentafluorobutyl)malononitrile | HCID 22234976 | 28% |
反応手順
Using 1.00 g of (4-chlorobenzyl)malononitrile, 10 ml of N,N-di-methylformamide, 0.21 g of sodium hydride (60% in oil), and 1.44 g of 4-iodo-1,1,1,2,2-pentafluorobutane, and according to the process described in the Production Example 1, there was obtained 0.47 g of 2-(4-chlorobenzyl)-2-(3,3,4,4,4-pentafluorobutyl)malononitrile (the present compound (23)).
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07011838B2 |
| 出典データセット | uspto-grants-2006_03 |
| ORD ID | ord-48f6f6ce0cb342d0882f91fafe4bb8db |
| 出典メモ | uspto-grants-2006_03 |