HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 786126, compound → HCID 22235013, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 786126 | HCID 786126 | — |
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 22235013 | HCID 22235013 | 80% |
Reaction Steps
Using 10.0 g of (3,4-difluorobenzyliden)malononitrile, 200 ml of ethanol and 0.6 g of sodium borohydride, and according to the process described in the REFERENCE PRODUCTION EXAMPLE 3, there was obtained 8.05 g of (3,4-difluorobenzyl)malononitrile (the intermediate (23)).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07011838B2 |
| Source dataset | uspto-grants-2006_03 |
| ORD ID | ord-dfe384726abe4c8ab7421ad2e3555df0 |
| Source note | uspto-grants-2006_03 |