HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 22234966, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 22235080 | HCID 22235080 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 22234966 | HCID 22234966 | 53% |
Reaction Steps
Using 10.0 g of (2-chloro-4-fluorobenzyliden)malononitrile, 200 ml of ethanol and 0.6 g of sodium borohydride, and according to the process described in the REFERENCE PRODUCTION EXAMPLE 3, there was obtained 0.55 g of (2-chloro-4-fluorobenzyl)malononitrile (the intermediate (24)).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07011838B2 |
| Source dataset | uspto-grants-2006_03 |
| ORD ID | ord-e2367ce57038457aa6072c0077b23abe |
| Source note | uspto-grants-2006_03 |