HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanol → (3-Benzyloxybenzyl)malononitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanol | HCID 702 | — |
| Reactant | Malononitrile | HCID 8010 | — |
| Reactant | 3-Benzyloxybenzaldehyde | HCID 74342 | — |
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Solvent | Water | HCID 962 | — |
| Product | (3-Benzyloxybenzyl)malononitrile | HCID 22235026 | 92% |
Reaction Steps
Using 1.06 g of 3-(benzyloxy)benzaldehyde, 0.33 g of malononitrile, 8 ml of ethanol, 1.5 ml of water and 57 mg of sodium borohydride, and according to the process described in the REFERENCE PRODUCTION EXAMPLE 19, there was obtained 1.20 g of (3-(benzyloxy)benzyl)malononitrile (the intermediate (31)).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07011838B2 |
| Source dataset | uspto-grants-2006_03 |
| ORD ID | ord-28a59cc287964bd9a7fe75163751483a |
| Source note | uspto-grants-2006_03 |