HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium borohydride → HCID 22235073, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium borohydride | HCID 4311764 | — |
| Reactant | HCID 22235079 | HCID 22235079 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 22235073 | HCID 22235073 | 96.3% |
Reaction Steps
Using 1.0 g of (2,6-dichloro-4-(trifluoromethyl)benzyliden)malononitrile, 20 ml of ethanol and 0.03 g of sodium borohydride, and according to the process described in the REFERENCE PRODUCTION EXAMPLE 3, there was obtained 0.97 g of (2,6-dichloro-4-(trifluoromethyl)benzyl)malononitrile (the intermediate (32)).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07011838B2 |
| Source dataset | uspto-grants-2006_03 |
| ORD ID | ord-4414c8bd01a3455195193ab283361bd6 |
| Source note | uspto-grants-2006_03 |