HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Amino-1-propene-1,1,3-tricarbonitrile → (E,E)-2-(1-Amino-2,2-dicyanoethenyl)-3-(4-nitrostyryl)acrylonitrile
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Amino-1-propene-1,1,3-tricarbonitrile | HCID 13356 | — |
| Reactant | 3-(4-Nitrophenyl)prop-2-enal | HCID 15614 | — |
| Product | (E,E)-2-(1-Amino-2,2-dicyanoethenyl)-3-(4-nitrostyryl)acrylonitrile | HCID 86588371 | — |
Reaction Steps
The compound was prepared as described in Example 3 by adding 4-nitrocinnamaldehyde (0.051 g, 0.29 mmol) to 2-amino-1-propene-1,1,3-tricarbonitrile (0.038 g, 0.29 mmol). After refluxing for 4 h and recrystallization from ethanol a yellow solid was obtained (0.08 g, 51%). The product gave the following analytical data:
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07012095B2 |
| Source dataset | uspto-grants-2006_03 |
| ORD ID | ord-6da3aaedad6445959b0b155d9cb2ea8e |
| Source note | uspto-grants-2006_03 |