HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19417624, compound → HCID 22228626, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19417624 | HCID 19417624 | — |
| Reactant | HCID 22228625 | HCID 22228625 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | HCID 22228626 | HCID 22228626 | 47% |
Reaction Steps
Ether cleavage of 108 mg of ethyl 4,6-dibromo-5-[3-(4-fluorobenzoyl)-4-methoxyphenoxy]-1-benzofuran-2-carboxylate with AlCl3/ethanethiol, in analogy with example . . . , yields 49 mg (47%) of ethyl 4,6-dibromo-5-[3-(4-fluorobenzoyl)-4-hydroxyphenoxy]-1-benzofuran-2-carboxylate.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07015246B2 |
| Source dataset | uspto-grants-2006_03 |
| ORD ID | ord-36ecfcbaccb6480a9af566e790c395e6 |
| Source note | uspto-grants-2006_03 |