3,4,5-Trichloronitrobenzene → HCID 22228178, compound

HRID 1744550Notes

Reaction equation

HRID 1744550 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([N+:10]([O-])=O)[CH:5]=[C:6]([Cl:9])[C:7]=1Cl.[O:13]1[CH2:18][CH2:17][N:16]([CH:19]2[CH2:24][CH2:23][NH:22][CH2:21][CH2:20]2)[CH2:15][CH2:14]1>>[Cl:9][C:6]1[CH:5]=[C:4]([CH:3]=[C:2]([Cl:1])[C:7]=1[N:22]1[CH2:23][CH2:24][CH:19]([N:16]2[CH2:17][CH2:18][O:13][CH2:14][CH2:15]2)[CH2:20][CH2:21]1)[NH2:10]

Participants

3

Reactant 2

HCID 883653,4,5-TrichloronitrobenzeneHCID 7957244-Morpholinopiperidine

Product 1

HCID 22228178HCID 22228178, compound

Procedure

By the reaction and treatment in the same manner as in Starting Material Synthesis Example 40 using 3,4,5-trichloronitrobenzene and 4-morpholinopiperidine, the title compound was obtained, melting point: 144–146° C.

Workup

  1. customBy the reaction and treatment in the same manner as

Sources & evidence

ORD record
ord-54363e4933814ee0a5c858c5502d9a89
Source dataset
uspto-grants-2006_03
Patent number
US07015218B1

Reaction notes

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